{"refrec":{"BRefID":238625,"RR":"<b>Shi, X.Z.; Song, S.Q.; Sun, A.L.; Liu, J.H.; Li, D.X.; Chen, J.</b> (2012). Rapid analysis of pyrethroid insecticides in aquaculture seawater samples via membrane-assisted solvent extraction coupled with gas chromatography-electron capture detection. <i>Analyst 137(2)</i>: 437-443. <a href=\"http://dx.doi.org/10.1039/c1an15782e\" target=\"_blank\">dx.doi.org/10.1039/c1an15782e</a>","BEntID":230312,"PublicFlag":1,"CheckedFlag":1,"wosflag":1,"vabbflag":null,"RefStringPartII":". <i>Analyst 137(2)</i>: 437-443. <a href=\"https://dx.doi.org/10.1039/c1an15782e\" target=\"_blank\">https://dx.doi.org/10.1039/c1an15782e</a>","DocTypID":8,"DocType":"Journal article","MarineFlag":0,"FreshFlag":0,"BrackishFlag":0,"TerrestrialFlag":0,"Authorstring":"Shi, X.Z.; Song, S.Q.; Sun, A.L.; Liu, J.H.; Li, D.X.; Chen, J.","OrigTitleTranslFlag":0,"Authorstringtrunc":"Shi, X.Z. <i>et al.</i>","Englishabstract":"A simple, efficient, and environmentally friendly membrane-assisted solvent extraction (MASE) method for the extraction and preconcentration of six pyrethroid insecticides from aquaculture seawater samples followed by gas chromatography-electron capture detection (GC-ECD) was successfully proposed. The operating conditions for MASE, such as the extraction solvent, solvent volume, NaCl concentration, stirring rate, extraction time, and temperature, were optimized. Compared to conventional Florisil-solid phase extraction (SPE), higher extraction recoveries (85.9% to 105.9%) of three spiked levels of the six pyrethroid pesticides in aquaculture seawater were obtained using MASE, and the RSD values were lower than 7.9%. The limits of detection (LOD, signal-to-noise ratio (S/N)=3) and quantification (LOQ, S/N = 10) were in the range of 0.037–0.166 and 0.12–0.55 µg L<sup>-1</sup>, respectively. The results demonstrate the excellent applicability of the MASE method in analyzing the six pyrethroid pesticides in aqueous samples. The proposed method exhibited a high potential for routine monitoring analysis of pyrethroid insecticides in seawater samples.","AbstractOtherLang":null,"BibLvlCode":"AS","StandardTitle":"Rapid analysis of pyrethroid insecticides in aquaculture seawater samples via membrane-assisted solvent extraction coupled with gas chromatography-electron capture detection","OrigTitleLangCode":"en","OrigTitleLangCodeExtended":"eng","OrigTitleLangID":15,"DateLastModified":{"date":"2024-12-10 01:33:17.368041","timezone_type":1,"timezone":"+01:00"},"UserAccessRight":null,"UserAccID":null,"AuthorKeywords":null,"OtherDescriptors":null,"Notes":null,"AnaPub":2012,"MonPub":null,"DateUpdate":"2015-10-28","DateCreate":"2014-05-18","SecASFANote":null,"ConfID":null,"PeerRev":1,"VlizCoreFlag":1,"WoScode":"WOS:000297998000023","VABBcode":null,"OpenAcc":1,"DOI":"10.1039/c1an15782e"},"refs":null,"anarec":{"AnaID":238625,"PubliDate":2012,"Pagination":"437-443","XtraPublOfAnaID":null,"ISBN":null,"Volume":"137","Issue":"2","BRefMon":null,"BRefMonRR":null,"BRefXtra":null,"BRefXtraRR":null,"SerBRefID":42098,"SerRR":"The Analyst. 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