{"refrec":{"BRefID":291641,"RR":"<b>Kotthoff, M.; Rüdel, H.; Jürling, H.</b> (2017). Detection of tetrabromobisphenol A and its mono- and dimethyl derivatives in fish, sediment and suspended particulate matter from European freshwaters and estuaries. <i>Anal. Bioanal. Chem. 409(14)</i>: 3685-3694. <a href=\"https://dx.doi.org/10.1007/s00216-017-0312-z\" target=\"_blank\">https://dx.doi.org/10.1007/s00216-017-0312-z</a>","BEntID":283684,"PublicFlag":1,"CheckedFlag":1,"wosflag":1,"vabbflag":1,"RefStringPartII":". <i>Anal. Bioanal. Chem. 409(14)</i>: 3685-3694. <a href=\"https://dx.doi.org/10.1007/s00216-017-0312-z\" target=\"_blank\">https://dx.doi.org/10.1007/s00216-017-0312-z</a>","DocTypID":8,"DocType":"Journal article","MarineFlag":1,"FreshFlag":1,"BrackishFlag":1,"TerrestrialFlag":0,"Authorstring":"Kotthoff, M.; Rüdel, H.; Jürling, H.","OrigTitleTranslFlag":0,"Authorstringtrunc":"Kotthoff, M. <i>et al.</i>","Englishabstract":"An analytical method was developed for the determination of tetrabromobisphenol A (TBBPA), 3,3′,5,5′-tetrabromobisphenol-A-monomethyl ether (MM-TBBPA) and 3,3′,5,5′-tetrabromobisphenol-A-dimethyl ether (DM-TBBPA), and its valid application on fish muscle matrix (bream and sole), suspended particulate matter (SPM) and surface sediment layer samples, using only 0.5 g sample material, is demonstrated. Here, for the first time, DM-TBBPA could be determined by an LC-MS/MS-based method applying atmospheric pressure photoionization (APPI), using the same sample extracts for all three analytes. Samplings covered freshwater fish (bream; annually, period 2007–2013) and SPM or sediment (every second year in the period 2008–2014) at selected European sites (rivers: Tees/UK, Mersey/UK, Western Scheldt/NL, Götaälv/SE, Rhône/FR; Lake Belau/DE). TBBPA could be quantified in 13 of 36 bream samples (range about 0.5–1.2 μg kg<sup>−1</sup> ww) and 7 of 7 sole muscle samples (range about 0.5–0.7 μg kg<sup>−1</sup> ww). Further, it could be quantified in 11 of the 14 SPM samples (range about 0.5–9.4 μg kg<sup>−1</sup> dw) and in both of the surface sediment layer samples (2.3–2.6 μg kg<sup>−1</sup> dw). MM-TBBPA could be quantified in 12 of 36 bream and 4 of 7 sole muscle samples (range about 0.8–1.8 μg kg<sup>−1</sup> ww). Further, it could be quantified in 10 of the 14 river SPM samples (range about 2.3–4.5 μg kg<sup>−1</sup> dw) and in both lake surface sediment layer samples (5.2–5.5 μg kg<sup>−1</sup> dw). DM-TBBPA was rarely detectable and could not be quantified above the limit of quantification in any sample.","AbstractOtherLang":null,"BibLvlCode":"AS","StandardTitle":"Detection of tetrabromobisphenol A and its mono- and dimethyl derivatives in fish, sediment and suspended particulate matter from European freshwaters and estuaries","OrigTitleLangCode":"en","OrigTitleLangCodeExtended":"eng","OrigTitleLangID":15,"DateLastModified":{"date":"2026-04-17 01:32:16.914135","timezone_type":1,"timezone":"+02:00"},"UserAccessRight":null,"UserAccID":null,"AuthorKeywords":"Brominated flame retardants Tetrabromobisphenol A Environmental monitoring Atmospheric pressure photoionization High-resolution mass spectrometry","OtherDescriptors":null,"Notes":null,"AnaPub":2017,"MonPub":null,"DateUpdate":"2018-02-13","DateCreate":"2018-01-04","SecASFANote":null,"ConfID":null,"PeerRev":1,"VlizCoreFlag":1,"WoScode":"WOS:000401408300018","VABBcode":null,"OpenAcc":1,"DOI":"10.1007/s00216-017-0312-z"},"refs":null,"anarec":{"AnaID":291641,"PubliDate":2017,"Pagination":"3685-3694","XtraPublOfAnaID":null,"ISBN":null,"Volume":"409","Issue":"14","BRefMon":null,"BRefMonRR":null,"BRefXtra":null,"BRefXtraRR":null,"SerBRefID":65810,"SerRR":"Analytical and Bioanalytical Chemistry. 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