Document of bibliographic reference 312352

BibliographicReference record

Type
Bibliographic resource
Type of document
Journal article
BibLvlCode
AS
Title
Elucidation of spirodactylone, a polycyclic alkaloid from the sponge Dactylia sp., and nonenzymatic generation from the co-metabolite Denigrin B
Abstract
Spirodactylone (1), a hexacyclic indolizidone alkaloid possessing a novel spiro ring system, was isolated from the marine sponge Dactylia sp. The structure was elucidated by extensive spectroscopic methods including application of the LR-HSQMBC NMR pulse sequence. Oxidative cyclization of denigrin B (2), an aryl-substituted 2-oxo-pyrroline derivative that was also isolated from the sponge extract, provided material identical to spirodactylone (1). This confirmed the assigned structure and provides insight into the probable biogenesis of 1.
WebOfScience code
https://www.webofscience.com/wos/woscc/full-record/WOS:000473116000075
Bibliographic citation
Kang, U.; Caldwell, D.R.; Cartner, L.K.; Wang, D.; Kim, C.-K.; Tian, X.; Bokesch, H.R.; Henrich, C.J.; Woldemichael, G.M.; Schnermann, M.J.; Gustafson, K.R. (2019). Elucidation of spirodactylone, a polycyclic alkaloid from the sponge Dactylia sp., and nonenzymatic generation from the co-metabolite Denigrin B. Organic Letters 21(12): 4750-4753. https://dx.doi.org/10.1021/acs.orglett.9b01636
Topic
Marine
Is peer reviewed
true

Authors

author
Name
Unwoo Kang
author
Name
Donald Caldwell
author
Name
Laura Cartner
author
Name
Dongdong Wang
Identifier
https://orcid.org/0000-0002-0412-6386
author
Name
Chang-Kwon Kim
author
Name
Xiangrong Tian
author
Name
Heidi Bokesch
author
Name
Curtis Henrich
author
Name
Girma Woldemichael
author
Name
Martin Schnermann
author
Name
Kirk Gustafson

Links

referenced creativework
type
DOI
accessURL
https://dx.doi.org/10.1021/acs.orglett.9b01636

Document metadata

date created
2019-07-02
date modified
2019-07-02